HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Cyanide → 2-Bromo-4-methoxy-5-(1-methylethoxy)benzene Acetonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Cyanide | HCID 9032 | — |
| Reactant | HCID 15514470 | HCID 15514470 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | 2-Bromo-4-methoxy-5-(1-methylethoxy)benzene Acetonitrile | HCID 11822156 | — |
Reaction Steps
1-Bromo-2-(chloromethyl)-5-methoxy-4-(1-methylethoxy)benzene (7.00 g, 23.8 mmol) and potassium cyanide (1.70 g, 26.1 mmol, freshly ground) are stirred in absolute DMSO (70 ml) for 12 hours at room temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07166588B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-31349d0fcb8b4b29a31ea9c10970201f |
| Source note | uspto-grants-2007_01 |