L-Lactic Acid → HCID 69507745, compound

HRID 1374564Notes

Reaction equation

HRID 1374564 reaction equation
Cl.[NH2:2][C@H:3]1[C:9](=[O:10])[N:8]([CH3:11])[C:7]2[CH:12]=[CH:13][CH:14]=[CH:15][C:6]=2[C:5]2[CH:16]=[CH:17][CH:18]=[CH:19][C:4]1=2.[C:20](O)(=[O:24])[C@H:21]([CH3:23])[OH:22]>>[OH:22][C@@H:21]([CH3:23])[C:20]([NH:2][C@H:3]1[C:9](=[O:10])[N:8]([CH3:11])[C:7]2[CH:12]=[CH:13][CH:14]=[CH:15][C:6]=2[C:5]2[CH:16]=[CH:17][CH:18]=[CH:19][C:4]1=2)=[O:24]

Participants

3

Reactant 2

HCID 107689L-Lactic AcidHCID 69508327HCID 69508327, compound

Product 1

HCID 69507745HCID 69507745, compound

Procedure

The title compound, MS: m/e=311.3 (M+H+), was prepared in analogy to example 1a) from (+)-(R)-7-amino-5-methyl-5H,7H-dibenzo[b,d]azepin-6-one hydrochloride and L-(+)-lactic acid.

Sources & evidence

ORD record
ord-5df490c916b54e8ca6fa6cd88e23ed80
Source dataset
uspto-grants-2007_01
Patent number
US07166587B2

Reaction notes

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