HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 21908404, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | HCID 69516577 | HCID 69516577 | — |
| Solvent | Sulfuric Acid | HCID 1118 | — |
| Product | HCID 21908404 | HCID 21908404 | 106.8% |
Reaction Steps
11.2 g of 2-ethoxy-3-[1-(2-chlorophenyl)-1-cyclopropyl]-acrylic acid is stirred in 230 ml of 1 M sulfuric acid and 42 ml of concentrated acetic acid for 24 hours at 110° C. Water is added, it is extracted with ethyl acetate, and ethyl acetate solution is washed with water. After drying (Na2SO4) and concentration by evaporation, 10.7 g of the product is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07166592B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-5c461acd69a940d3b19df576ccb6cfa6 |
| Source note | uspto-grants-2007_01 |