HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-butyl N-[(2-chloro-5-nitrophenyl)methyl]carbamate → Tert-butyl (5-amino-2-chlorobenzyl)carbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-butyl N-[(2-chloro-5-nitrophenyl)methyl]carbamate | HCID 21077620 | — |
| Catalyst | Platinum | HCID 23939 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Tert-butyl (5-amino-2-chlorobenzyl)carbamate | HCID 21077619 | — |
Reaction Steps
Prepared from 3-(tert.butyloxycarbonylaminomethyl)-4-chloro-nitrobenzene by hydrogenation in methanol at ambient temperature in the presence of platinum on charcoal, melting point: 75–77° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07166599B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-c357a77e43484c8b8c8b986ae6c1f80f |
| Source note | uspto-grants-2007_01 |