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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1374642Generated: October 31, 2026

Phosphorus oxychloride → 4-Chloro-2-(methylthio)-5-phenylpyrimidine

https://huagongshe.com/reaction/1374642

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPhosphorus oxychlorideHCID 24813—
ReactantHCID 178503405HCID 178503405—
Product4-Chloro-2-(methylthio)-5-phenylpyrimidineHCID 11020900—

Reaction Steps

Prepared from 2-methylsulphenyl-4-hydroxy-5-phenyl-pyrimidine by reacting with phosphorus oxychloride at reflux temperature, melting point: 99° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07166599B2
Source datasetuspto-grants-2007_01
ORD IDord-5d2ea9fe1d664d15b2251f51cf780d22
Source noteuspto-grants-2007_01