HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 21077597, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | 4-Chloro-2-(methylthio)-5-phenylpyrimidine | HCID 11020900 | — |
| Reactant | Dichloromethane methanol | HCID 21226129 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21077597 | HCID 21077597 | — |
Reaction Steps
Prepared from 2-methylsulphenyl-4-chloro-5-phenyl-pyrimidine by reacting with methylamine in ethanol at 90° C., Rf value: 0.63 (silica gel; methylene chloride/methanol=20:1)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07166599B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-431fdcfd98004bca8946444124ab1364 |
| Source note | uspto-grants-2007_01 |