HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 21077591, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | 4,5-Dichloro-2-(methylsulfanyl)pyrimidine | HCID 14270850 | — |
| Reactant | Cyclohexane ethylacetate | HCID 21867204 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21077591 | HCID 21077591 | — |
Reaction Steps
Prepared from 2-methylsulphenyl-4,5-dichloro-pyrimidine by reacting with methylamine in ethanol at 90° C., melting point: 241° C., Rf value: 0.59 (silica gel; cyclohexane/ethyl acetate=2:1)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07166599B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-221370aad7494892ae7fc36e4c63fac3 |
| Source note | uspto-grants-2007_01 |