HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21077591, compound → HCID 21077605, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21077591 | HCID 21077591 | — |
| Reactant | Dichloromethane methanol | HCID 21226129 | — |
| Reactant | Acetic acid--water (1/1) | HCID 21899381 | — |
| Reactant | Sodium periodate | HCID 23667635 | — |
| Product | HCID 21077605 | HCID 21077605 | — |
Reaction Steps
Prepared from 2-methylsulphenyl-4-methylamino-5-chloro-pyrimidine by reacting with sodium periodate in glacial acetic acid/water, Rf value: 0.50 (silica gel; methylene chloride/methanol=9:1)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07166599B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-3bcdf901c46b474eabfbfdca33fd70f4 |
| Source note | uspto-grants-2007_01 |