HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 21077593, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | 4-Chloro-5-methoxy-2-(methylsulfanyl)pyrimidine | HCID 243511 | — |
| Reactant | Cyclohexane ethylacetate | HCID 21867204 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21077593 | HCID 21077593 | — |
Reaction Steps
Prepared from 2-methylsulphenyl-4-chloro-5-methoxy-pyrimidine by reacting with methylamine in ethanol at 90° C., Rf value: 0.22 (silica gel; cyclohexane/ethyl acetate=2:1)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07166599B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-f9e56a004e814f4ab48b651c6fa6e567 |
| Source note | uspto-grants-2007_01 |