Methylamine → HCID 21077593, compound

HRID 1374646Notes

Reaction equation

HRID 1374646 reaction equation
[CH3:1][S:2][C:3]1[N:8]=[C:7](Cl)[C:6]([O:10][CH3:11])=[CH:5][N:4]=1.[CH3:12][NH2:13].C1CCCCC1.C(OCC)(=O)C>C(O)C>[CH3:1][S:2][C:3]1[N:8]=[C:7]([NH:13][CH3:12])[C:6]([O:10][CH3:11])=[CH:5][N:4]=1

Participants

5

Reactant 3

HCID 6329MethylamineHCID 2435114-Chloro-5-methoxy-2-(methylsulfanyl)pyrimidineHCID 21867204Cyclohexane ethylacetate

Product 1

HCID 21077593HCID 21077593, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Prepared from 2-methylsulphenyl-4-chloro-5-methoxy-pyrimidine by reacting with methylamine in ethanol at 90° C., Rf value: 0.22 (silica gel; cyclohexane/ethyl acetate=2:1)

Sources & evidence

ORD record
ord-f9e56a004e814f4ab48b651c6fa6e567
Source dataset
uspto-grants-2007_01
Patent number
US07166599B2

Reaction notes

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