HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 241191, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | Dichloromethane methanol | HCID 21226129 | — |
| Reactant | 4-Chloro-5-methyl-2-(methylthio)pyrimidine | HCID 23562708 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 241191 | HCID 241191 | — |
Reaction Steps
Prepared from 2-methylsulphenyl-4-chloro-5-methyl-pyrimidine by reacting with methylamine in ethanol at 100° C., melting point: 134° C., Rf value: 0.35 (silica gel; methylene chloride/methanol=40:1)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07166599B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-33e661c97a374a4ba36280217621b54d |
| Source note | uspto-grants-2007_01 |