Methylamine → HCID 241191, compound

HRID 1374647Notes

Reaction equation

HRID 1374647 reaction equation
[CH3:1][S:2][C:3]1[N:8]=[C:7](Cl)[C:6]([CH3:10])=[CH:5][N:4]=1.[CH3:11][NH2:12].C(Cl)Cl.CO>C(O)C>[CH3:1][S:2][C:3]1[N:8]=[C:7]([NH:12][CH3:11])[C:6]([CH3:10])=[CH:5][N:4]=1

Participants

5

Reactant 3

HCID 6329MethylamineHCID 21226129Dichloromethane methanolHCID 235627084-Chloro-5-methyl-2-(methylthio)pyrimidine

Product 1

HCID 241191HCID 241191, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Prepared from 2-methylsulphenyl-4-chloro-5-methyl-pyrimidine by reacting with methylamine in ethanol at 100° C., melting point: 134° C., Rf value: 0.35 (silica gel; methylene chloride/methanol=40:1)

Sources & evidence

ORD record
ord-33e661c97a374a4ba36280217621b54d
Source dataset
uspto-grants-2007_01
Patent number
US07166599B2

Reaction notes

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