HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → 2-Methylsulphinyl-4-methylamino-5-methyl-pyrimidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | HCID 241191 | HCID 241191 | — |
| Reactant | Dichloromethane methanol | HCID 21226129 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 2-Methylsulphinyl-4-methylamino-5-methyl-pyrimidine | HCID 21077601 | — |
Reaction Steps
Prepared from 2-methylsulphenyl-4-methylamino-5-methyl-pyrimidine by reacting with 3-chloro-peroxybenzoic acid in methylene chloride, Rf value: 0.23 (silica gel; methylene chloride/methanol/ conc. aqueous ammonia=20:1:0.1)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07166599B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-ede1d5379e934237a600435a4149b0e6 |
| Source note | uspto-grants-2007_01 |