HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 21077592, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | 4-Chloro-5-fluoro-2-(methylsulfanyl)pyrimidine | HCID 15709298 | — |
| Reactant | Dichloromethane methanol | HCID 21226129 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21077592 | HCID 21077592 | — |
Reaction Steps
Prepared from 2-methylsulphenyl-4-chloro-5-fluoro-pyrimidine by reacting with methylamine in ethanol at 100° C., Rf value: 0.53 (silica gel; methylene chloride/methanol/conc. aqueous ammonia=20:1:0.1)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07166599B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-8c1dd1ec030548ec9ef91a43a4b1c6a1 |
| Source note | uspto-grants-2007_01 |