HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 178491700, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Ethyl formate | HCID 8025 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 15626815 | HCID 15626815 | — |
| Reactant | HCID 21115369 | HCID 21115369 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 178491700 | HCID 178491700 | — |
Reaction Steps
Prepared from methyl 4-methoxybenzylsulphenyl-acetate and ethyl formate in the presence of sodium and subsequent reaction with S-methylisothiourea-sulphate in ethanol, Rf value: 0.4 (silica gel; methylene chloride/methanol/conc. aqueous ammonia=20:1:0.1)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07166599B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-7acc21edd9444c9f933ae87cc1097a05 |
| Source note | uspto-grants-2007_01 |