m-Chloroperbenzoic acid → HCID 21077598, compound

HRID 1374651Notes

Reaction equation

HRID 1374651 reaction equation
[CH3:1][S:2][C:3]1[N:8]=[C:7]([NH:9][CH3:10])[C:6]([N+:11]([O-:13])=[O:12])=[C:5]([NH:14][CH3:15])[N:4]=1.ClC1C=CC=C(C(OO)=[O:24])C=1>C(Cl)Cl.CO>[CH3:1][S:2]([C:3]1[N:4]=[C:5]([NH:14][CH3:15])[C:6]([N+:11]([O-:13])=[O:12])=[C:7]([NH:9][CH3:10])[N:8]=1)=[O:24]

Participants

4

Reactant 2

HCID 70297m-Chloroperbenzoic acidHCID 21077589HCID 21077589, compound

Product 1

HCID 21077598HCID 21077598, compound

Reagents, catalysts & solvents 1

HCID 21226129Dichloromethane methanolSolvent

Procedure

Prepared from 2-methylsulphenyl-4,6-bis(methylamino)-5-nitro-pyrimidine by reacting with m-chloroperbenzoic acid, Rf value: 0.36 (silica gel; methylene chloride/methanol=3:1)

Sources & evidence

ORD record
ord-2e6385e416774be1b009e9a6e7b36501
Source dataset
uspto-grants-2007_01
Patent number
US07166599B2

Reaction notes

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