m-Chloroperbenzoic acid → HCID 21077602, compound

HRID 1374652Notes

Reaction equation

HRID 1374652 reaction equation
[CH3:1][S:2][C:3]1[N:8]=[C:7]([NH:9][CH3:10])[C:6]([N+:11]([O-:13])=[O:12])=[C:5]([NH2:14])[N:4]=1.ClC1C=CC=C(C(OO)=[O:23])C=1>>[CH3:1][S:2]([C:3]1[N:8]=[C:7]([NH:9][CH3:10])[C:6]([N+:11]([O-:13])=[O:12])=[C:5]([NH2:14])[N:4]=1)=[O:23]

Participants

3

Reactant 2

HCID 70297m-Chloroperbenzoic acidHCID 21077594HCID 21077594, compound

Product 1

HCID 21077602HCID 21077602, compound

Procedure

Prepared from 2-methylsulphenyl-4-methylamino-5-nitro-6-amino-pyrimidine by reacting with m-chloro-perbenzoic acid, melting point: 229–234° C.

Sources & evidence

ORD record
ord-e146e65b013846558ea414aec4b6b6d5
Source dataset
uspto-grants-2007_01
Patent number
US07166599B2

Reaction notes

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