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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1374667Generated: October 31, 2026

Hydrochloric Acid → HCID 69414094, compound

https://huagongshe.com/reaction/1374667

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 44305340HCID 44305340—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 69414094HCID 69414094—

Reaction Steps

Under cooling with ice, a solution of 4N solution of hydrogen chloride in dioxane (12 ml) was added dropwise to the compound prepared in Example 2 (1180 mg). The solution was warmed to room temperature and stirred for 1 hour. The reaction mixture was concentrated to give the title compound (920 mg) having the following physical data.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07166590B2
Source datasetuspto-grants-2007_01
ORD IDord-a7d2b0c4971f4a4b8d4b362323dc3dba
Source noteuspto-grants-2007_01