HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 69414094, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 44305340 | HCID 44305340 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 69414094 | HCID 69414094 | — |
Reaction Steps
Under cooling with ice, a solution of 4N solution of hydrogen chloride in dioxane (12 ml) was added dropwise to the compound prepared in Example 2 (1180 mg). The solution was warmed to room temperature and stirred for 1 hour. The reaction mixture was concentrated to give the title compound (920 mg) having the following physical data.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07166590B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-a7d2b0c4971f4a4b8d4b362323dc3dba |
| Source note | uspto-grants-2007_01 |