Salicylaldehyde → HCID 17839128, compound

HRID 1374843Notes

Reaction equation

Br[CH2:2][CH2:3][CH2:4][O:5][CH:6]1[CH2:11][CH2:10][CH2:9][CH2:8][O:7]1.[CH:12](=[O:20])[C:13]1[C:14](=[CH:16][CH:17]=[CH:18][CH:19]=1)[OH:15]>>[O:7]1[CH2:8][CH2:9][CH2:10][CH2:11][CH:6]1[O:5][CH2:4][CH2:3][CH2:2][O:15][C:14]1[CH:16]=[CH:17][CH:18]=[CH:19][C:13]=1[CH:12]=[O:20]

Participants

Reactant 2

HCID 6998Salicylaldehyde

HCID 27779882-(3-Bromopropoxy)tetrahydro-2H-pyran

Product 1

HCID 17839128HCID 17839128, compound

Procedure

By using 2-(3-bromopropoxy)tetrahydro-2H-pyran and salicylaldehyde, the title compound was obtained as colorless oil by similar procedures to those of Example 60b (yield: quantitative).

Sources & evidence

ORD record: ord-5ab40e497a9e431696a4a19a07ae5430
Source dataset: uspto-grants-2007_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07166617B2

Reaction notes

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