HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Phenylimidazolidin-2-one → HCID 17839083, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Phenylimidazolidin-2-one | HCID 255273 | — |
| Reactant | (2-Bromoethoxy)-tert-butyldimethylsilane | HCID 3608067 | — |
| Product | HCID 17839083 | HCID 17839083 | — |
Reaction Steps
By using 1-phenylimidazolidin-2-one obtained by the method described in literature (J. Org. Chem., 1951, 16, 1829) and t-butyldimethylsilyl 2-bromoethyl ether obtained by the method of Example 92a, 1-[2-(t-butyldimethylsilyloxy)ethyl]-3-phenylimidazolidin-2-one was obtained as crude product by similar procedures to those of Example 151a. By using the resulting product, the title compound was obtained as colorless solid by similar procedures to those of Example 92b (yield: 75%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07166617B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-084a8b07edec4ea5b2383dd7e30c7713 |
| Source note | uspto-grants-2007_01 |