Phenylboronic Acid → HCID 69264461, compound

HRID 1375062Notes

Reaction equation

HRID 1375062 reaction equation
[C:1]1(B(O)O)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[NH2:10][C:11]1[CH:15]=[C:14](Cl)[S:13][C:12]=1[S:17]([NH2:20])(=[O:19])=[O:18]>>[NH2:10][C:11]1[CH:15]=[C:14]([C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)[S:13][C:12]=1[S:17]([NH2:20])(=[O:19])=[O:18]

Participants

3

Reactant 2

HCID 66827Phenylboronic AcidHCID 109559343-Amino-5-chlorothiophene-2-sulfonamide

Product 1

HCID 69264461HCID 69264461, compound

Procedure

The title compound was prepared from phenylboronic acid and 3b by following the procedure in example 3c. This compound is a white solid: MS (ES) 255 (M+H)+; 1H NMR (400 MHz, CD3OD)δ7.61 (m, 2 H), 7.42–7.37 (m, 3 H), 6.89 (s, 1H).

Sources & evidence

ORD record
ord-0c1ada4a1d47410faff145241161642d
Source dataset
uspto-grants-2007_01
Patent number
US07166639B2

Reaction notes

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