HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → HCID 10104678, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | Ethyl bromoacetate | HCID 7748 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Sodium acetylacetonate hydrate | HCID 6008486 | — |
| Product | HCID 10104678 | HCID 10104678 | — |
Reaction Steps
10 g of sodium acetylacetonate and 20 g of potassium carbonate in 50 ml of acetone were heated to reflux and 15 g of bromoacetic acid ethyl ester was added dropwise over 15 minutes. After refluxing for several days, the solid was filtered off and washed with petroleum ether and acetone. Fractional distillation yielded 6.4 g of 5-acetyl-6-oxo-heptanoic acid ethyl ester.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07166648B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-fd4f3659e30945a68019c7444405d454 |
| Source note | uspto-grants-2007_01 |