HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Acrylate → Methyl 4-acetyl-5-oxohexanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Acrylate | HCID 7294 | — |
| Reactant | Acetylacetone | HCID 31261 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Product | Methyl 4-acetyl-5-oxohexanoate | HCID 281668 | — |
Reaction Steps
4-acetyl-5-oxohexanoic acid methyl ester was prepared through the Michael addition of methyl acrylate to acetyl acetone in the presence of metallic sodium. The crude product was purified by vacuum distillation and received in a purity of approximately 99%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07166648B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-8d22ed37bdee427c8a0568662258ebb2 |
| Source note | uspto-grants-2007_01 |