HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86589523, compound → HCID 69023190, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86589523 | HCID 86589523 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 69023190 | HCID 69023190 | 96% |
Reaction Steps
To a solution of 2-benzyloxycarbonylamino-5-butyryloxyphenylbutanoate (KCBG04) KCBG04 (0.05 g, 0.12 mmol) in MeOH (5 mL) was added Pd/C (10%, 4 mg) at room temperature. After stirring for 20 min under H2, the reaction mixture was filtered and evaporated in vacuo to give 2-amino-5-butyryloxyphenyl butanoate (KCBG06, 0.031 g, 96%) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07166744B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-fc64397badbf427b8d33c5cba1585dcb |
| Source note | uspto-grants-2007_01 |