HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-[[4-(Diethylaminocarbonyl)phenyl]amino]-4-(methylamino)-5-nitropyrimidine → 5-Amino-2-[[4-(diethylaminocarbonyl)phenyl]amino]-4-(methylamino)pyrimidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-[[4-(Diethylaminocarbonyl)phenyl]amino]-4-(methylamino)-5-nitropyrimidine | HCID 58786799 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | 5-Amino-2-[[4-(diethylaminocarbonyl)phenyl]amino]-4-(methylamino)pyrimidine | HCID 58786782 | — |
Reaction Steps
Hydrogenation of 2-[[4-(diethylaminocarbonyl)phenyl]amino]-4-(methylamino)-5-nitropyrimidine (from Example 2(3) above) over Pd/C gave the title compound as a solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07169778B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-0be54c0d505d46f39df47f3887c0f4f1 |
| Source note | uspto-grants-2007_01 |