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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1375477Generated: October 30, 2026

Potassium Carbonate → HCID 21897138, compound

https://huagongshe.com/reaction/1375477

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
Reactant6-chloro-N-(3-chloro-4-methoxyphenyl)-N'-cycloheptyl-[1,3,5]triazine-2,4-diamineHCID 21897021—
SolventMethanolHCID 887—
ProductHCID 21897138HCID 21897138—

Reaction Steps

To 6-chloro-N-(3-chloro-4-methoxyphenyl)-N′-cycloheptyl-[1,3,5]triazine-2,4-diamine (5 g) dissolved in methanol was added K2CO3 (3.2 g) and refluxed for about 6–8 h. TLC was monitored. After the completion of the reaction, the reaction mass was filtered through vacuum and the filtrate was evaporated to yield the title compound. (Wt. 4.7 g Y: 95%)

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07169784B2
Source datasetuspto-grants-2007_01
ORD IDord-6dfb8cb579e74cf388326681cf9ba921
Source noteuspto-grants-2007_01