HCID 69507945, compound → HCID 10250245, compound

Participants

Reaction Steps

The titled compound was prepared according to the procedure described in Example 1F, substituting the ester from Example 1E for the ester from Example 3C. MS (ESI(+)) m/e 399 (M+H)+; 1H NMR (300 MHz, DMSO-d6) δ 9.96 (s, 1H), 7.30 (s, 1H), 7.25 (t, J=8.4 Hz, 1H), 7.18 (t, J=8.4 Hz, 1H), 7.08–7.14 (m, 2H), 6.78 (dt, J=6.9, 1.5 Hz, 1H), 6.55 (d, J=5.8 Hz, 1H), 6.51 (d, J=5.8 Hz, 1H), 4.12 (t, J=5.7 Hz, 2H), 3.70 (s, 3H), 3.6–3.3 (overlapping m, 2H).

Provenance & Evidence