HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 9819702, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 58787775 | HCID 58787775 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 9819702 | HCID 9819702 | — |
Reaction Steps
1.67 g (0.005 mol) of (3E)-4-[3-(cyclopentyloxy)-4-methoxyphenyl]-3-(methoxycarbonyl)-3-butenoic acid are suspended in 8 ml of methylene chloride. 0.36 ml of N,N-DMF (0.005 mol), are added under stirring at room temperature, the solution is cooled to 0° C. and 0.87 ml (0.01 mol) of oxalyl chloride is added.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07169808B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-281e6350ec764e808916a08394ccfdb3 |
| Source note | uspto-grants-2007_01 |