HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69425740, compound → HCID 58787872, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69425740 | HCID 69425740 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 58787872 | HCID 58787872 | — |
Reaction Steps
Acetic acid 4-acetoxy-2-acetoxymethyl-2-acetylamino-4-biphenyl-4-yl-butyl ester (5 mmol) is dissolved in EtOH (50 mL) and hydrogenated at atmospheric pressure using 10% Pd-C (10%) at room temperature for 12 h. After filtration and concentration, the crude product is obtained as a white solid and used in the next step without further purification. MS: (ES+): 398.2 (M+1)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07169817B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-9923d13ff2d942aab2b518e9e60e3d2f |
| Source note | uspto-grants-2007_01 |