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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1375918Generated: November 1, 2026

HCID 69425740, compound → HCID 58787872, compound

https://huagongshe.com/reaction/1375918

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 69425740HCID 69425740—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 58787872HCID 58787872—

Reaction Steps

Acetic acid 4-acetoxy-2-acetoxymethyl-2-acetylamino-4-biphenyl-4-yl-butyl ester (5 mmol) is dissolved in EtOH (50 mL) and hydrogenated at atmospheric pressure using 10% Pd-C (10%) at room temperature for 12 h. After filtration and concentration, the crude product is obtained as a white solid and used in the next step without further purification. MS: (ES+): 398.2 (M+1)+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07169817B2
Source datasetuspto-grants-2007_01
ORD IDord-9923d13ff2d942aab2b518e9e60e3d2f
Source noteuspto-grants-2007_01