HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexyl isocyanate → HCID 11948029, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexyl isocyanate | HCID 18502 | — |
| Reactant | 1-Pyrrolidinepropanamine | HCID 31670 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 11948029 | HCID 11948029 | — |
Reaction Steps
In an argon atmosphere 10 mmol of cyclohexylisocyanate was added slowly to 10 mmol of 1-(3-aminopropyl)pyrrolidine in 10 ml of acetonitrile. The product precipitated instantly as a pure white solid. The solvent was removed under reduced pressure and the product was crystallized with oxalic acid from diethyl ether/ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07169928B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-8a9b0449871541a8b0372ee48ea48a42 |
| Source note | uspto-grants-2007_01 |