HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 9860014, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2-Chlorobenzothiazole | HCID 11987 | — |
| Reactant | N-(2-Aminoethyl)piperidine | HCID 33944 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 9860014 | HCID 9860014 | — |
Reaction Steps
2-Chlorobenzothiazole (10 mmol), 10 mmol of 2-piperidinoethanamine, and 30 mmol of triethylamine in 50 ml of dry ethanol were refluxed for 6 hours. The product was crystallized with hydrochloric acid in 2-propanol and recrystallized in methanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07169928B2 |
| Source dataset | uspto-grants-2007_01 |
| ORD ID | ord-304cfb96d86843a8a1bf53d1f13d3401 |
| Source note | uspto-grants-2007_01 |