HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 86751196, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Fumaric Acid | HCID 444972 | — |
| Reactant | HCID 67575787 | HCID 67575787 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86751196 | HCID 86751196 | — |
Reaction Steps
1.73 g of 6-(2-imidazolinylamino)-5-methylbenzodioxan and 0.861 g of fumaric acid are dissolved in 20 mL of methanol. The solution is heated and treated with about 20 mL of ether. After cooling, the crystals which formed are collected and found to be 2.14 g of 6-(2-imidazolinylamino)-5-methylbenzodioxan fumarate salt, which melts at 199°-201° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05663189 |
| Source dataset | uspto-grants-1997_09 |
| ORD ID | ord-e80aee952c514a029adba49deb4b4ddb |
| Source note | uspto-grants-1997_09 |