HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylenediamine → HCID 54423976, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylenediamine | HCID 3301 | — |
| Reactant | HCID 21840490 | HCID 21840490 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 54423976 | HCID 54423976 | — |
Reaction Steps
To a solution of 0.205 g of ethylenediamine in 1 mL of methylene chloride is added dropwise a solution of 0.13 g of 7-methyl-6-isothiocyanato-2,3-dihydrobenzofuran in 2 mL of methylene chloride. The mixture is stirred at room temperature for 1 hour and evaporated to provide 6-[N'-(2-aminoethyl)thioureido]-7-methyl-2,3-dihydrobenzofuran as the crude product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05663189 |
| Source dataset | uspto-grants-1997_09 |
| ORD ID | ord-0dd62e915fe74e6ab39714231bc57090 |
| Source note | uspto-grants-1997_09 |