HCID 15428311, compound → HCID 15379550, compound

Participants

Reaction Steps

0.211 g of the 3-hydroxymethylimidazo[5,1-b]thiazole prepared in Preparation 55 was suspended in 20 ml of dichloromethane. To this suspension was added 1.1 g of manganese dioxide, and the mixture was stirred at room temperature for 16 hours. The reaction solution was filtered, and then concentrated to dryness under reduced pressure to give 0.146 g (yield 71%) of the title compound.

Provenance & Evidence