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HRID1376684

反应详情

EQUATION

反应方程式

HRID 1376684 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)OC(=O)N[C@@H](Cc1ccc(C#N)cc1)C(=O)O
HCID7020841

Boc-L-4-Cyanophenylalanine

C15H18N2O4

结构：CC(C)[C@H](NC(=O)[C@H](CC(=O)OC(C)(C)C)NC(=O)CN)C(=O)OC(C)(C)C
HCID15674413

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)OC(C)C.CCOC(C)=O
HCID22281796

未命名化合物

收率 66%

PROCEDURE

实验过程

By coupling rac N-Boc-3-(p-cyanophenyl)alanine (French Published Specification 2593 814) and H-Gly-Asp(OtBu)-Val-OtBu there is obtained [N-Boc-3-(p-cyanophenyl)-DL-alanyl]-Gly-Asp(OtBu)-Val-OtBu, m.p. 140°-145° C. from ethyl acetate/isopropyl ether, yield: 66%.