HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 178426708, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 178426711 | HCID 178426711 | — |
| Product | HCID 178426708 | HCID 178426708 | 100.1% |
Reaction Steps
To 135 g of 1-(2-methyl-5-nitrophenyl)guanidine nitrate (Japanese Unexamined Patent Publication (Kokai) No. 6-87834), 21 g of sodium hydroxide in 1.0 L of a cold aqueous solution was directly added, followed by stirring at room temperature for 10 minutes. The crystals were filtered, sufficiently washed with water and then forced-air dried at 60° C. to obtain 102 g of the objective compound as pale yellow crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07728131B2 |
| Source dataset | uspto-grants-2010_06 |
| ORD ID | ord-fa0ea5bd65864cb187b6153359d0c746 |
| Source note | uspto-grants-2010_06 |