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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1376853Generated: October 31, 2026

2-Methoxypropene → 4-[(1-Methoxy-1-methyl-ethoxyimino)-methyl]-pyridine

https://huagongshe.com/reaction/1376853

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-MethoxypropeneHCID 8300—
Reactant4-Pyridinecarbaldehyde oximeHCID 12764—
SolventDichloromethaneHCID 6344—
Product4-[(1-Methoxy-1-methyl-ethoxyimino)-methyl]-pyridineHCID 54535369—

Reaction Conditions

Temperature60 °C

Reaction Steps

1.5 ml of 2-methoxy-propene were added all at once to a suspension of 610 mg of pyridine-4-aldoxime in 10 ml of methylene chloride and the mixture was stirred for 18 hours at 60° C. under reduced pressure. The mixture was cooled and evaporated to dryness under reduced pressure to obtain 950 mg of 4-[(1-methoxy-1-methyl-ethoxyimino)-methyl]-pyridine.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05663164
Source datasetuspto-grants-1997_09
ORD IDord-4c5a2ac97a544e49949dc727a88070c0
Source noteuspto-grants-1997_09