HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Ethyl Ketone → Benzoic Acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Ethyl Ketone | HCID 6569 | — |
| Reactant | p-Fluorotoluene | HCID 9603 | — |
| Reactant | HCID 131720182 | HCID 131720182 | — |
| Catalyst | Cobalt(II) acetate tetrahydrate | HCID 61372 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | Benzoic Acid | HCID 243 | — |
Reaction Steps
Para-Fluorotoluene derivatives B16 are heated at about 90° C. to 110° C. for about 2-3 hours with cobalt diacetate-tetrahydrate and ethyl methyl ketone in acetic acid under pressure of oxygen-butane to produce benzoic acid derivatives B1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05663448 |
| Source dataset | uspto-grants-1997_09 |
| ORD ID | ord-0e091eeb4f194b19a0d50530c648c37b |
| Source note | uspto-grants-1997_09 |