HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 86751213, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | N-(2-bromo-4-tert-butylphenyl)acetamide | HCID 258026 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86751213 | HCID 86751213 | — |
Reaction Steps
A solution of 24.33 g (90 mmol) of N-acetyl-2-bromo-4-tert-butyl aniline in 73.5 ml of 95% ethanol and 46 ml of concentrated hydrochloric acid is heated under reflux one hour. Then the mixture is cooled and the product is filtered, washed with cold 95% ethanol and dried. The yield of title compound is 21.75 g (91%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05663448 |
| Source dataset | uspto-grants-1997_09 |
| ORD ID | ord-5875059ff93643f683c83cfc2abc72d8 |
| Source note | uspto-grants-1997_09 |