HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22913882, compound → HCID 22913582, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22913882 | HCID 22913882 | — |
| Reactant | HCID 178455851 | HCID 178455851 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 22913582 | HCID 22913582 | — |
Reaction Steps
50 ml (0.13 mols) of a THF solution of 2.5M of propylmagnesium bromide was dropped in a mixed solution of 44.5 g (0.1 mol) of 1-chloro-1-phenyl-4-(4-(3,5-difluoro-4-difluoromethoxyphenyl)butyl)-1-silacyclohexane and 300 ml of THF. After ordinary after-treatments, 4-(4-(3,5-difluoro-4-difluoromethoxyphenyl)butyl)-1-phenyl-1-propyl-1-silacyclohexane was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05665271 |
| Source dataset | uspto-grants-1997_09 |
| ORD ID | ord-1786171af10b4aaf8e98a2eabf15a4ec |
| Source note | uspto-grants-1997_09 |