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HRID1377481

反应详情

EQUATION

反应方程式

HRID 1377481 的结构方程式

REACTANTS

反应物

2
结构：[BH4-].[Na+]
HCID4311764

Sodium borohydride (Na(BH4))

H4BNa

结构：Cc1cccc(NC(=O)OC(C)(C)C)c1CNc1cccn2c(C=O)c(C)nc12
HCID23294184

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cccc(NC(=O)OC(C)(C)C)c1CNc1cccn2c(CO)c(C)nc12
HCID23287290

未命名化合物

收率 79.6%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CO
溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

The title compound is prepared according to the procedure described for example 2 starting from 8-(2-tert-Butoxycarbonylamino-6-methylbenzylamino)-3-formyl-2-methylimidazo[1,2-a]pyridine (0.15 g) and sodium borohydride (15 mg) in methanol. 0.12 g of the title compound of m.p. 102°-104° C. are isolated.

WORKUP

后处理

  1. customThe title compound is prepared