HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22915168, compound → HCID 22915173, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22915168 | HCID 22915168 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22915173 | HCID 22915173 | 108.8% |
Reaction Steps
A solution of 4-(3-benzyloxy-5-fluorophenyl)-4-methoxytetrahydrofuran (1.1 g) in ethanol (20 ml) was hydrogenated in the presence of 10% palladium-on-charcoal catalyst (1 00 mg) for about 3 hours. The mixture was filtered and the filtrate was evaporated to give 840 mg of the title compound. m.p. 136°-137° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05665749 |
| Source dataset | uspto-grants-1997_09 |
| ORD ID | ord-87dfc3ec3e00434e81cc44fe5e04f708 |
| Source note | uspto-grants-1997_09 |