N-bromobutanimide → HCID 22915172, compound

HRID 1377595Notes

Reaction equation

HRID 1377595 reaction equation
[CH3:1][N:2]1[C:6](=[O:7])[C:5]2[CH:8]=[C:9]([CH3:12])[CH:10]=[CH:11][C:4]=2[S:3]1(=[O:14])=[O:13].[Br:15]N1C(=O)CCC1=O>C(Cl)(Cl)(Cl)Cl>[CH3:1][N:2]1[C:6](=[O:7])[C:5]2[CH:8]=[C:9]([CH2:12][Br:15])[CH:10]=[CH:11][C:4]=2[S:3]1(=[O:13])=[O:14]

Participants

4

Reactant 2

HCID 67184N-bromobutanimideHCID 13330822HCID 13330822, compound

Product 1

HCID 22915172HCID 22915172, compound

Reagents, catalysts & solvents 1

HCID 5943Carbon TetrachlorideSolvent

Procedure

A solution of 2,5-dimethyl-1,1-dioxo-benzo[d]isothiazole-3-one (5.8 g) in carbon tetrachloride (100 ml) containing 2,2-azo-bis(2-methyl-propionitrile) (50 mg) and 4.8 g of N-bromosuccinimide was heated at reflux for about 2 hours.

Workup

  1. temperaturewas heated
  2. temperatureat reflux for about 2 hours

Sources & evidence

ORD record
ord-c76e4fe2e52045a68c50232cc3db5906
Source dataset
uspto-grants-1997_09
Patent number
US05665749

Reaction notes

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