HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → HCID 22915172, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 13330822 | HCID 13330822 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 22915172 | HCID 22915172 | — |
Reaction Steps
A solution of 2,5-dimethyl-1,1-dioxo-benzo[d]isothiazole-3-one (5.8 g) in carbon tetrachloride (100 ml) containing 2,2-azo-bis(2-methyl-propionitrile) (50 mg) and 4.8 g of N-bromosuccinimide was heated at reflux for about 2 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05665749 |
| Source dataset | uspto-grants-1997_09 |
| ORD ID | ord-c76e4fe2e52045a68c50232cc3db5906 |
| Source note | uspto-grants-1997_09 |