Allylamine → HCID 178457594, compound

HRID 1377893Notes

Reaction equation

HRID 1377893 reaction equation
[ClH:1].[C:2]([NH:5][C:6](=[NH:9])OC)(=[NH:4])[NH2:3].[CH2:10]([NH2:13])[CH:11]=[CH2:12]>C(O)C>[ClH:1].[CH2:10]([NH:13][C:6]([NH:5][C:2]([NH2:4])=[NH:3])=[NH:9])[CH:11]=[CH2:12]

Participants

4

Reactant 2

HCID 7853AllylamineHCID 178496818HCID 178496818, compound

Product 1

HCID 178457594HCID 178457594, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Into 3 ml of ethanol were dissolved 5 g of guanyl-O-methylisourea hydrochloride and 3 ml of allylamine. The resulting solution was reacted at room temperature for 24 hours in a nitrogen stream. The reaction mixture was then filtered and the precipitates were washed with ethanol to give 3.14 g of allylbiguanide hydrochloride as needle like crystals (m.p.: 178°-179° C.).

Workup

  1. customThe resulting solution was reacted at room temperature for 24 hours in a nitrogen stream
  2. filtrationThe reaction mixture was then filtered
  3. washthe precipitates were washed with ethanol

Sources & evidence

ORD record
ord-f4a5fceb7d3d46e0900136496b5df6fd
Source dataset
uspto-grants-1997_09
Patent number
US05665843

Reaction notes

Loading…