Ammonia → HCID 22915513, compound

Participants

Reaction Steps

The desired compound was prepared according to the method of Example 15, step 4, except substituting N-benzyloxy-4-[4-(4-cyanophenyl)phenyl]butyramide, prepared as in step 1, for N-benzyloxy-4-[3-(4-fluorophenyl)phenoxyl]butyramide. 1H NMR (DMSO-d6) δ 1.82 (m, 2H), 1.99 (t, 2H, J=8 Hz), 2.62 (t, 2H, J=7 Hz), 7.33 (d, 2H, J=9 Hz), 7.69 (d, 2H, J=9 Hz), 7.89 (m, 4H), 8.68 (s, 1H), 10.38 (s, 1H). MS (DCI/NH3) 298 (M+NH4+, 80), 280 (M+H+, 75), 236 (100).

Provenance & Evidence