HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl isocyanate → HCID 54046895, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl isocyanate | HCID 62412 | — |
| Reactant | 3-Fluoropyridine | HCID 67794 | — |
| Reactant | Lithium diisopropylamide | HCID 2724682 | — |
| Reactant | HCID 178506753 | HCID 178506753 | — |
| Product | HCID 54046895 | HCID 54046895 | — |
Reaction Steps
Following the procedure of Gribble and Saulnier, Tetrahedron Lett., 21:4137-4140 (1980)) reacting 3-fluoropyridine (Aldrich) with LDA and reacting the 3-fluoro-4-lithiopyridine intermediate with t-butyl isocyanate, the title compound was prepared.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05668141 |
| Source dataset | uspto-grants-1997_09 |
| ORD ID | ord-50c8f29eb80c4451a9815b50eaf4fff6 |
| Source note | uspto-grants-1997_09 |