Hydrochloric Acid → HCID 67622582, compound
Reaction equation
C([O:3][C:4]([CH:6]1[CH2:11][CH2:10][N:9]([CH:12]2[CH2:21][CH2:20][C:19]3[C:14](=[CH:15][CH:16]=[CH:17][CH:18]=3)[CH2:13]2)[CH2:8][CH2:7]1)=[O:5])C.[ClH:22]>>[ClH:22].[CH2:13]1[C:14]2[C:19](=[CH:18][CH:17]=[CH:16][CH:15]=2)[CH2:20][CH2:21][CH:12]1[N:9]1[CH2:10][CH2:11][CH:6]([C:4]([OH:5])=[O:3])[CH2:7][CH2:8]1Participants
3
Procedure
Ethyl-1-(tetralin-2-yl)piperdine-4-carboxylate (7.1 g, 0.025 mol) was treated with 6N HCl (80 ml) at room temperature. After stirring overnight, the suspension was filtered off and the solid dried in vacuo to yield 1-(tetralin-2-yl)piperdine-4-carboxylic acid hydrochloride salt.
Workup
- filtrationthe suspension was filtered off
- customthe solid dried in vacuo
Sources & evidence
- ORD record
- ord-7f232976da524787a3387e0fad629b25
- Source dataset
- uspto-grants-1997_09
- Patent number
- US05668148
Reaction notes
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