Hydrochloric Acid → HCID 67622582, compound

HRID 1378498Notes

Reaction equation

HRID 1378498 reaction equation
C([O:3][C:4]([CH:6]1[CH2:11][CH2:10][N:9]([CH:12]2[CH2:21][CH2:20][C:19]3[C:14](=[CH:15][CH:16]=[CH:17][CH:18]=3)[CH2:13]2)[CH2:8][CH2:7]1)=[O:5])C.[ClH:22]>>[ClH:22].[CH2:13]1[C:14]2[C:19](=[CH:18][CH:17]=[CH:16][CH:15]=2)[CH2:20][CH2:21][CH:12]1[N:9]1[CH2:10][CH2:11][CH:6]([C:4]([OH:5])=[O:3])[CH2:7][CH2:8]1

Participants

3

Procedure

Ethyl-1-(tetralin-2-yl)piperdine-4-carboxylate (7.1 g, 0.025 mol) was treated with 6N HCl (80 ml) at room temperature. After stirring overnight, the suspension was filtered off and the solid dried in vacuo to yield 1-(tetralin-2-yl)piperdine-4-carboxylic acid hydrochloride salt.

Workup

  1. filtrationthe suspension was filtered off
  2. customthe solid dried in vacuo

Sources & evidence

ORD record
ord-7f232976da524787a3387e0fad629b25
Source dataset
uspto-grants-1997_09
Patent number
US05668148

Reaction notes

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