HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 178503998, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | (3-Fluorophenyl)thiourea | HCID 2734799 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178503998 | HCID 178503998 | — |
Reaction Steps
A mixture of 3-fluorophenylthiourea (20.0 g, 166.7 mmol) and methyl iodide (24.8 g, 175.0 mmol) in 300 ml of ethanol is stirred at RT for 2 days. It is then heated to reflux for 30 min., cooled and stripped of solvent to give S-methyl-3-fluorophenylisothiourea hydroiodide, an orange solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05670456 |
| Source dataset | uspto-grants-1997_09 |
| ORD ID | ord-950b836463ff495eabd5a1f448773a22 |
| Source note | uspto-grants-1997_09 |