1,2-Ethanediamine, N1,N1,N2-trimethyl- → HCID 22909007, compound

Participants

Reaction Steps

Substantially the same procedure as in Example 2 was repeated using 500 mg (0.98 mmol) of Compound 1 obtained in Example 1 and 0.62 mi (4.9 mmol) of N,N,N'-trimethyl-ethylenediamine. The resulting crude crystals were recrystallized from cyclohexane/toluene to give 280 mg (yield 48%) of Compound 6 as yellow needles.

Provenance & Evidence